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1 article(s) from Fanelli, Flavio

Contribution of microreactor technology and flow chemistry to the development of green and sustainable synthesis

Flavio Fanelli,
Giovanna Parisi,
Leonardo Degennaro and
Renzo Luisi

Beilstein J. Org. Chem. 2017, 13, 520–542, doi:10.3762/bjoc.13.51

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Graphical Abstract

Figure 1: Microreactor technologies and flow chemistry for a sustainable chemistry.

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Scheme 1: A flow microreactor system for the generation and trapping of highly unstable carbamoyllithium spec...

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Scheme 2: Flow synthesis of functionalized α-ketoamides.

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Scheme 3: Reactions of benzyllithiums.

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Scheme 4: Trapping of benzyllithiums bearing carbonyl groups enabled by a flow microreactor. (Adapted with pe...

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Scheme 5: External trapping of chloromethyllithium in a flow microreactor system.

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Scheme 6: Scope for the direct tert-butoxycarbonylation using a flow microreactor system.

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Scheme 7: Control of anionic Fries rearrangement reactions by using submillisecond residence time. (Adapted w...

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Figure 2: Chip microreactor (CMR) fabricated with six layers of polyimide films. (Reproduced with permission ...

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Scheme 8: Flow microreactor system for lithiation, borylation, Suzuki–Miyaura coupling and selected examples ...

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Scheme 9: Experimental setup for the flow synthesis of 2-fluorobi(hetero)aryls by directed lithiation, zincat...

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Scheme 10: Experimental setup for the coupling of fluoro-substituted pyridines. (Adapted with permission from [53]...

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Scheme 11: Continuous flow process setup for the preparation of 11 (Reproduced with permission from [54], copyrigh...

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Scheme 12: Continuous-flow photocatalytic oxidation of thiols to disulfides.

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Scheme 13: Trifluoromethylation by continuous-flow photoredox catalysis.

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Scheme 14: Flow photochemical synthesis of 6(5H)-phenanthridiones from 2-chlorobenzamides.

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Scheme 15: Synthesis of biaryls 14a–g under photochemical flow conditions.

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Scheme 16: Flow oxidation of hydrazones to diazo compounds.

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Scheme 17: Synthetic use of flow-generated diazo compounds.

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Scheme 18: Ley’s flow approach for the generation of diazo compounds.

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Scheme 19: Iterative strategy for the sequential coupling of diazo compounds.

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Scheme 20: Integrated synthesis of Bakuchiol precursor via flow-generated diazo compounds.

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Scheme 21: Kappe’s continuous-flow reduction of olefines with diimide.

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Scheme 22: Multi-injection setup for the reduction of artemisinic acid.

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Scheme 23: Flow reactor system for multistep synthesis of (S)-rolipram. Pumps are labelled a, b, c, d and e; L...

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Figure 3: Reconfigurable modules and flowcharts for API synthesis. (Reproduced with permission from [85], copyrig...

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Figure 4: Reconfigurable system for continuous production and formulation of APIs. (Reproduced with permissio...

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Review

Published 14 Mar 2017

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